It has to be Derrick Jefferson's KO of Maurice Harris in 6. The sickest KO I have ever seen, ever. Was a good scrap, too. Both fighters were down. Harris had Jefferson wobbled up to the time he got KO'd. Dramatic finish:
See highlights: https://www.youtube.com/watch?v=z81taPNIkw8
Honourable mention:
Mike Tyson's KO of Marvis Frazier in 1. Just sickening the uppercut Frazier got before he was brutally finished off.
David Tua's KO of, you guessed it, John Ruiz in 1. Tua didn't need to give him that left uppercut on the way down. He was already out. Glad Ruiz wasn't seriously hurt by that.
Rafael Pineda KO's Roger Mayweather in 9. Talk about being anesthetized.
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